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Pyrolysis is a thermal decomposition process of organic material at elevated temperatures in an anaerobic environment. It involves the cleavage of large complex molecules into smaller, more analytically useful fragments by the thermal energy.

As an analogy, a Mass Spectrometer shatters compounds using electron impact, the compound is fragmented in a reproducible way, the ions are separated by the MS and the result is a spectrum which is both qualitative and quantitative. Pyrolysis works in much the same way. By applying heat to a sample that is comparable to the energy of specific bonds, the molecule will fragment in a reproducible way. The fragments are then separated by the analytical column to produce the chromatogram (pyrogram) which contains both qualitative and quantitative information. The number of peaks, the resolution by capillary GC, and the relative intensities of the peaks permit discrimination among many similar formulations, making pyrolysis a powerful tool in the identification of unknown samples.

CDS Analytical released the first commercial analytical pyrolyzer (Model 100) in late 60s, and has been proudly making world's best pyrolyzers for over 50 years. Our products have evolved through 6 generations and represent; the industries highest standard.​

CDS pyrolyzers can be used in universities, forensic labs, labs, government settings, and more for all your polymer research needs. They are also compatible with all major brands of GC/MS including: Agilent, Bruker, Thermo, PerkinElmer, and Shimadzu.

Available models

Programmable time's
0 - 999.9 minutes
Trap
No
Temperature range
Up to 1300°C
Temperature accuracy
1°C
Heating rate
0.01°C/ms to 20°C/ms 0.01°C/sec to 999.9°C/sec 0.01°C/min to 999.9°C/min
Probe clean
Yes
Probe dry
Yes
Multi-temperature steps
No
Interface type
Low thermal mass
Interface temperature
Up to 350°C
Interface heating rate
1°C/min to 100°C/min
GC Connection
Injection port direct mount
Dimension (W x H x D)
25 x 44 x 46 cm

CDS's most cost effective single temperature Pyroprobe.

The CDS Model 4000 Pyroprobe is specifically designed for users that occasionally need pryolysis to assist their work. The 4000 has an economical price tag, and possesses a direct GC injection port mount feature to simplify the operation and installation. Installation and removal only takes minutes on conventional GC. 

Key features

  • CDS resistively heated filament
  • Super compact design with small foot print
  • Compatible to all major GC through remote start cable
  • Direct GC injection port mount
  • Sample rack for easy sample storage
  • Compatible with the CDS Thermal Desorption probe
  • USB connectivity
  • Powerful PC interface
  • Quick connect cables
DISC Technology
Standard
Trap
No
Temperature range
Up to 1300°C
Temperature accuracy
1°C
Heating rate
0.01°C/ms to 20°C/ms 0.01°C/sec to 999.9°C/sec 0.01°C/min to 999.9°C/min
RSD
1.5% (Polystyrene)
Multi-temperature steps
Yes, Up to 10 temperature profiles. Allows for multiple thermal desorption or pyrolysis steps on each sample
GC Connection
Heated Transfer line (up to 350°C)
Dimension (W x H x D)
381 X 292 X 406 mm
Weight
16.3 kg
Options
Autosampler, 1/2" Coil Probe, 1/4" Ribbon Probe, 1/4" Coil Probe

CDS's 6th Generation Pyroprobe with up to 10 programmed temperature steps

​The CDS Model 6150 Pyroprobe is the basic model of CDS's 6th generation Pyroprobe. The 6150 is equipped with Drop-In-Sample-Chamber (DISC) technology with easy sample loading and 1.5% RSD. The system connects to any model GC with a heated sample line for easy on/off installation. 

Key features

  • Equipped with CDS DISC System
  • Easy sample prep
  • The DISC system brings an amazing 1.5% RSD for 5 run pyrolysis of Polystyrene at 600 °C by holding 0.1 °C temperature accuracy and calibrated temperature precision.
  • Superior resolution: The system could reach C55 for pyrolyzing Polyethylene through GC with a single quad mass-spec.
  • Newly designed oven with high temperature valve
  • Windows 10 compatible software
  • Built-In leak check
  • Remote GC start
  • Easy maintenance
  • Powerful library
DISC Technology
Standard
Trap
Standard Tenax-TA
Temperature range
Up to 1300°C
Temperature accuracy
0.1°C
Reactant gas
Standard
Heating rate
0.01°C/ms to 20°C/ms 0.01°C/sec to 999.9°C/sec 0.01°C/min to 999.9°C/min
Multi-temperature steps
Yes, Up to 10 temperature profiles. Allows for multiple thermal desorption or pyrolysis steps on each sample
GC Connection
Heated Transfer line (up to 350°C)
Dimension (W x H x D)
381 X 292 X 406 mm
Weight
17.5 kg
Options
Autosampler, Thermal Desorption Tube Module, Dynamic Headspace Module, External Reactor Module, Cryotrap (-180°C), Cryofocuser (-180°C), 1/4" and 1/2" Manual Probe, Electronic Mass Flow Controller (N2, O2, Air, CO2, He Calibrated)

CDS's 6th Generation Pyroprobe with up to 10 programmed temperature steps​.

The CDS Model 6200 Pyroprobe adds in an analytical trap to enable collecting analytes using slow rate pyrolysis. The built-in trap also expands the capability to use a reactant gas (like oxygen and air), and perform thermal desorption on sorbent tubes or larger samples. The 6200 also permits direct pyrolysis to the GC in GC carrier gas. The 6200 is equipped with Drop-In-Sample-Chamber (DISC) technology with easy sample loading and 1.5% RSD. 

Key features

  • Equipped with CDS DISC System
  • Easy sample prep
  • The DISC system brings an amazing 1.5% RSD for 5 run pyrolysis of Polystyrene at 600 °C by holding 0.1 °C temperature accuracy and calibrated temperature precision.
  • Analytical focus trap with pre-heat and pre-desorb
  • Superior resolution:  A heating temperature of 350 °C assures minimum carry over.
  • Thermal desorption and dynamic headspace
  • Built-In leak check
  • Remote GC start
  • Easy maintenance
  • Powerful library
Temperature range
Programmable to 1300°C
Heating rate
Programmable from 0.01°C/s to 20°C/s
Interface temerature
From ambient up to 300°C
Compatibility
6150, 6200
Dimension (W x H x D)
381 X 292 X 406 mm
Weight
4" X 5" X 3"
Options
Autosampler

CDS's DISC module provides the easiest way to load your pyroloysis sample. 

The Drop-In-Sample-Chamber (DISC) is a novel accessory module for the 6000 series Pyroprobes. It transforms the horizontal sample loading probe used in traditional manual pyrolysis system to a convenient vertical loading system. The DISC saves your precious time by reducing the sample tube loading process. When used with the filler rod, the DISC helps to reduce sample preparation time by skipping the quartz wool insertion. The DISC chamber also isolates the pyrolysis sample tube from touching the platinum heating coil and can help to eliminate coil damages.  

Key features

  • CDS resistively heated filament
  • Most convenient way to load pyrolysis samples
  • Minimum effort in routine maintenance
  • Upgrade to autosmapler 
  • Optical window
  • Software compatible
Programmable time's
0 - 999.9 minutes
Trap
Yes, Standard Tenax-TA Cryotrap available
Temperature range
Up to 1400°C
Temperature accuracy
1°C
Heating rate
0.01°C/ms to 20°C/ms 0.01°C/sec to 999.9°C/sec 0.01°C/min to 999.9°C/min
Probe clean
Yes. User-selectable.
Probe dry
Yes. User-selectable.
System max pressure
500 PSI (3.4 MPa)
Reactor max temperature
800°C
Catalyst volume
6 X 75 mm (2 ml total volume)
Interface type
Low thermal mass
Interface temperature
Up to 350°C
Interface heating rate
1°C/min to 100°C/min
GC Connection
Heated Transfer line (up to 350°C)
Dimension (W x H x D)
280 X 670 X 480 mm
Weight
25 kg

CDS's HPR Pyroprobe allows pyrolysis at elevated pressure with built-in reactor.​

The CDS HPR Pyroprobe enables users to study both high temperature and pressure in a micro-scale environment, with the convenience of results sent directly to their GC/MS. The unit is built on 5200 platform with a backpressure regulator and heated catalyst bed. Samples can be pyrolyzed at max 500 PSI (3400 kPa), passed through a user-selectable catalyst bed, and collected onto the built-in trap. 

Key features

  • CDS resistively heated filament
  • Pyrolysis in extreme enviroments
  • User selectable catalyst reactor
  • Digital display of the pressure and temperature
  • Heavy duty back pressure regulator
  • Optional steam module
Wavelength
260 - 400 nm
Light intensity
800 mW/mm2
Light control
0-100% (1% step)
Temperature accuracy
1°C
Compatibility
6150, 6200 with Autosampler
Dimension (W x H x D)
4" X 5" X 3"
Weight
1 kg
Options
Calibration sensor

Photoprobe is a device that irradiates sample in the Drop In Sample Chamber with high intensity UV light

The CDS Photoprobe is a unique device that uses high power xenon lamp to irradiate sample in the Drop In Sample Chamber (DISC) to introduce environmental degradation with the combination of programmable temperature and user-select reactant gas. The intensity of the UV light is 100 times stronger than any competitor’s product, which shortens the testing time from hours to minutes.

Key features

  • High power xenon lamp
  • Free space focusing
  • 260 nm - 400 nm wavelength
  • Easy installation
  • UV light safety
  • Software compatible
  • Aerospace
  • Agriculture
  • Automotive
  • Biopharmaceutical and Biotechnology
  • Chemical
  • Construction
  • Cosmetics & Personal Care
  • Defense
  • Die & Mould
  • Education & Academics
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  • Energy
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  • Food & Beverage
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  • Railway
  • Semiconductor, Solar & Electronics
  • Service
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  • Wholesale & Retail
CDS AnalyticalCDS Analytical is a leading global provider of innovative thermal sample preparation instrumentation for the analytical laboratory. For over 35 years our exclusive focus has been on conceiving, designing, manufacturing, and supporting leading edge instruments. CDS offers a complete suite of diverse front-end GC equipment including pyrolyzers, purge and trap, headspace, and thermal desorption systems. These robust, field-tested products provide the entire range of temperature, heating rate, and multiple step manipulations required by today's most demanding analytical laboratories. With a well-established leadership role with pyrolyzers and other introduction systems, as well as broad market penetration on a global scale, CDS continues to be innovative and dynamic, and will pioneer the next wave of sample introduction instrumentation.
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